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James T. Nurmi; Vaishnavi Sarathy; Paul G. Tratnyek; Donald R. Baer; James E. Amonette; Abhi Karkamkar(Profiled Authors: James Nurmi; Paul Tratnyek)
Journal of Nanoparticle Research. 2011;13(5):1937-1952.Abstract
Most methods currently being used to recover Fe0-core/oxide-shell nanoparticles from solutions (including the solvents they are synthesized or stored in) are potentially problematic because they may alter the particle composition (e.g., depositing salts formed from solutes) or leave the particles prone to transformations during subsequent storage and handling (e.g., due to residual moisture). In this study, several methods for recovery of nanoparticles from aqueous solution were studied to determine how they affect the structure and reactivity of the recovered materials. Simple washing of the nanoparticles during vacuum filtration (i.e., "flash drying") can leave up to ∼17 wt% residual moisture. Modeling calculations suggest this moisture is mostly capillary or matric water held between particles and particle aggregates, which can be removed by drying for short periods at relative vapor pressures below 0.9. Flash drying followed by vacuum drying, all under N
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